SODIUM PICOSULPHATE
 

MOLECULAR WEIGHT: 499.4 MOLECULAR FORMULA: C18H13N Na2O8S2 , H2 O

SODIUM PICOSULPHATE

TESTS EP
CHARACTERS

A white or almost white, crystalline powder, freely soluble in water, slightly soluble in alcohol, practically insoluble in ether.

IDENTIFICATION
IR

UV

TEST C

TEST D

TEST FOR SODIUM


Infrared absorption spectrophotometry to compare with the spectrum obtained with sodium picosulfate CRS.

Ultraviolet absorption: should confirm with reference standard.

white precipitate is formed with barium chloride solution.

A violet colour develops with sulphuric acid and potassium dichromate solution.

The solution gives reaction of sodium .

APPEARANCE OF SOLUTION

Solution S is clear and not more intensely coloured than reference solution GY7.

ACIDITY OR ALKLALINITY

Not more than 0.25 ml of 0.01 M sodium hydroxide is required for neutralization.

RELATED SUBSTANCE

Examine by thin-layer chromatography. NMT 0.2 %

CHLORIDES

NMT 200ppm

SULPHATES

NMT 400ppm

HEAVY METALS

NMT 20ppm

WATER

3.0% to 5.0 %w/w

ASSAY

98.5% to 100.5% w/w

 

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