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TESTS |
EP |
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CHARACTERS |
A white or almost white, crystalline powder, freely soluble in water, slightly soluble in alcohol, practically insoluble in ether. |
IDENTIFICATION
IR
UV
TEST C
TEST D
TEST FOR SODIUM
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Infrared absorption spectrophotometry to compare with the spectrum obtained with sodium picosulfate CRS.
Ultraviolet absorption: should confirm with reference standard.
white precipitate is formed with barium chloride solution.
A violet colour develops with sulphuric acid and potassium dichromate solution.
The solution gives reaction of sodium .
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APPEARANCE OF SOLUTION |
Solution S is clear and not more intensely coloured than reference solution GY7.
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ACIDITY OR ALKLALINITY |
Not more than 0.25 ml of 0.01 M sodium hydroxide is required for neutralization. |
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RELATED SUBSTANCE |
Examine by thin-layer chromatography. NMT 0.2 % |
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CHLORIDES
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NMT 200ppm |
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SULPHATES
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NMT 400ppm |
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HEAVY METALS
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NMT 20ppm |
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WATER
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3.0% to 5.0 %w/w |
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ASSAY
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98.5% to 100.5% w/w |